ONH836系列:氧氮?dú)浞治鰞x(熔融法)
軟件特點(diǎn)和優(yōu)勢
Cornerstone氧氮?dú)浞治鲕浖殖?個(gè)主要部分:分析、診斷、設(shè)定、儀器,界面可以快速導(dǎo)航和組織。工具條、滑動(dòng)條和下拉式菜單簡化了校正和數(shù)據(jù)處理的參數(shù)設(shè)定。分析軟件同時(shí)包括實(shí)時(shí)的環(huán)境參數(shù)的監(jiān)測,提供完整的系統(tǒng)圖表模擬。高級(jí)診斷程序包括全數(shù)字化的在線操作手冊(cè)、維護(hù)模擬演示、圖片說明等提供快速指導(dǎo)。Cornerstone氧氮?dú)浞治鲕浖瑫r(shí)支持***的數(shù)據(jù)文檔格式和可變的報(bào)告格式。 采用三個(gè)**的紅外器檢測氧含量,同時(shí)檢測CO和CO2,然后在轉(zhuǎn)化為CO2集中檢測。美國分析儀廠家直銷
Procedure - Solid Samples
Determine the instrument blank.
Repeat steps 2b through 2g a minimum of three times.
Set the blank following the procedure outlined in the operator's instruction manual.
Instrument calibration/drift correction.
Login a minimum of 3 Standard replicates.
Weigh approximately *** grams of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.
Note: LECO Reference Materia***o not require preparation.See preparation statement on the reference material certificate.
LECO分析儀優(yōu)惠價(jià)格雙直流風(fēng)扇保證持續(xù)冷卻,不受電壓波動(dòng)的影響。
Procedure - Solid Samples
Prepare the instrument as outlined in the operator's instruction manual.
Determine the instrument blank.
Login a minimum of 3 Blank replicates.
Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Place a 502-344 Nickel Basket into the loading head.
Note: samples using automation should be placed in the appropriate autoloader position before starting the
analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.
Sample Preparation
Sampling and sample preparation of refractory metals such as titanium and zirconium is somewhat different from that of steel. Unlike steel samples, hydrogen is not as mobile in this group of materials; therefore, storage in liquid nitrogen or dry ice is not required. However, it is important to keep the sample cool when cutting or sectioning. Sample preparation for oxygen and nitrogen determination has beendifferent from that of hydrogen determination.
工具條、滑動(dòng)條和下拉式菜單簡化了校正和數(shù)據(jù)處理的參數(shù)設(shè)定。
氧氮?dú)浞治鰞x的原理:分析樣品在惰性氣流存在下于石墨坩堝中加熱熔融,其中脈沖爐溫度可自由設(shè)定,并通過一個(gè)非接觸式的光學(xué)溫度傳感器進(jìn)行實(shí)時(shí)監(jiān)控,用于實(shí)現(xiàn)樣品的完全分解,反應(yīng)所生成的CO H2和N2被帶入到具有高穩(wěn)定性和靈敏度的檢測系統(tǒng)進(jìn)行檢測。對(duì)于CO的檢測采用的是非色散性紅外檢測器,對(duì)于N2和H2的檢測則采用熱導(dǎo)檢測器。
氧氮?dú)浞治鰞x的特點(diǎn):快速準(zhǔn)確分析,自動(dòng)化操作;精密氣體校準(zhǔn);CO紅外檢測器,高分辨率和重現(xiàn)性的N、H熱導(dǎo)池檢測器;同一臺(tái)儀器實(shí)現(xiàn)熔融提取和熱提?。粺崽崛》治鰰r(shí)間可調(diào);可自由選擇溫度*高達(dá)2500 °C;光學(xué)溫度計(jì)溫度測定和控制;所有檢測器自動(dòng)調(diào)零/自動(dòng)水平控制(ALC);數(shù)據(jù)評(píng)估的自動(dòng)優(yōu)化選擇范圍;爐自動(dòng)清潔和坩堝自動(dòng)進(jìn)樣(可選);外設(shè)電腦進(jìn)行操作和控制;樣品信息保存; 所有樣品數(shù)據(jù)可追蹤查詢;通過FTP或本地局域網(wǎng)進(jìn)行數(shù)據(jù)傳輸; ON,H分析輕松切換。
強(qiáng)力內(nèi)循環(huán)水冷裝置。安徽元素分析儀供應(yīng)商
提供各種無機(jī)材料、鋼鐵、有色金屬、硬質(zhì)合金陶瓷材料中寬范圍的氧氮?dú)渫瑫r(shí)測定。美國分析儀廠家直銷
氧氮?dú)浞治鰞x的常見故障及解決方法
供電正常、通訊正常,點(diǎn)擊確認(rèn)鍵后分析儀不工作。這是沒有水流,爐子溫度太高或儀器通道電壓不正常。如沒有水流,爐子溫度太高這些信息會(huì)顯示在顯示器畫面上,但沒有信息顯示說明這兩項(xiàng)正常。接下來檢查儀器通道零位電壓,如果比±3V高出1V以上,可能是因?yàn)闅馄靠樟耍蛘呤强諝膺M(jìn)入到分析儀中。檢查并更換化學(xué)試劑,如果有空氣進(jìn)入熱導(dǎo)池里,熱導(dǎo)池的電壓就會(huì)<-6V,此時(shí)打開右面的門,堵住爐子氣體進(jìn)口,10s后,熱導(dǎo)池電壓值必然升高。經(jīng)過逐一排查,**終確認(rèn)堿石棉有問題,更換后儀器正常。 美國分析儀廠家直銷