專業(yè)元素分析儀

來源: 發(fā)布時(shí)間:2022-01-08

氧氮?dú)浞治鰞x的常見故障及解決方法:氧和氮空白值超過20。這是由于氣流小,不能將爐子中的空氣驅(qū)趕出去??烧{(diào)節(jié)氣體流量,調(diào)節(jié)載氣壓力在0.2~0.4MPa。接通儀器載氣,放一個(gè)石墨坩堝在下電極上,打開主電源開關(guān),點(diǎn)擊軟件上的關(guān)爐按鈕,關(guān)閉爐子并等待10s。調(diào)節(jié)流量調(diào)節(jié)器,直到流量計(jì)a顯示為30L/h,打開爐子。調(diào)節(jié)調(diào)節(jié)器直到流量計(jì)b顯示為50L/h,再次關(guān)閉爐子。如果以上設(shè)置不穩(wěn)定,則增加流量至100L/h,反復(fù)調(diào)節(jié)直至儀器穩(wěn)定。試樣加載過程中完全密閉,消除大氣的中可能帶來的雜質(zhì)的污染。專業(yè)元素分析儀

專業(yè)元素分析儀,分析儀

SummaryThedeterminationoftheamountofoxygen,nitrogen,andhydrogeniniron,steel,nickel-,andcobalt-basealloysrepresentssomeofthemostimportantqualitymetricsforthesematerials.Oxygenisusedtocreatesteelfrompigironbyremovingexcesscarbon.Oxygencontentmustbecontrolledtolimittheamountofcarbonmonoxidethatcanbeformedduringsolidificationwhichmaycauseexcessiveporosity.Nitrogenisconsideredbothanimpurityaswellasanimportantalloyingagent.Itcanbepresentasanitrideorinterstitiallyinitsgaseousform.Increasednitrogencontentisknowntoincreaseyieldandtensilestrength,thusdecreasingductilityandformability.Excessivelevelsmayevolveduringsolidificationthusincreasingporosity.Highhydrogencontentistheprimarycauseofembrittlement,blisteringandflakingduetoitshighmobilitythroughthelatticeandprovidesnopotentialalloyingbenefits.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.新疆美國LECO分析儀多少錢20位或100位全自動分析系統(tǒng)。

專業(yè)元素分析儀,分析儀

氧氮?dú)浞治鰞x的常見故障及解決方法儀器啟動時(shí)顯示。沒有水流。系統(tǒng)分析電流切斷,分析停止。這是水流探測器不正常,水泵不工作,管道堵塞。將儀器的右面板取下,觀察水流探測器,用手?jǐn)D壓補(bǔ)水塑料水瓶,發(fā)現(xiàn)水流正常,顯示正常,證明水流探測器正常,管道暢通。啟動循環(huán)水泵,但分析儀顯示沒有水流,此時(shí)可判定水泵不正常。打開水泵轉(zhuǎn)子密封口,啟動泵發(fā)現(xiàn)電機(jī)正常運(yùn)轉(zhuǎn),此時(shí)關(guān)閉進(jìn)水,拆下水泵,發(fā)現(xiàn)葉輪脫落。經(jīng)了解,判定是由于外部冷卻水停水,儀器內(nèi)循環(huán)水溫過高(水溫應(yīng)≤70℃),致使葉輪(葉輪材料PVC)熱脹并脫軸。用粘合劑粘合葉輪后再粘于葉輪軸上,待粘合劑凝固后試車,儀器運(yùn)行正常。

MethodSelectionTwomethodsaredescribedinthisapplicationnote;eithermethodcanbeusedtoanalyzeiron,steel,nickel-,andcobalt-basealloys.ThePrecisionMethodisrecommendedforgeneraluseandwillprovidethebestprecisionandaccuracythroughoutthetypicalO,N,andHconcentrationsfoundinthisgroupofmetals;approximatecycletimeis3.5minutes.TheFastTrackmethodcanbeusedwherespeedofanalysisisacriticalcomponent;forexample,whenmoltenmetalisbeingsampledandresultsarerequiredintheshortestpossibletime.Thismethodwillproducesuitableresultsformostsamples;approximatecycletimeis2.25minutes.Asnotedabove,samplingandsamplepreparationarekeyelementstoaccurateO,N,andHdeterminationaswell.Itisuptotheusertodeterminewhichmethodbestmeetstheirneeds.減少了繁瑣的額外數(shù)據(jù)處理。

專業(yè)元素分析儀,分析儀

Procedure-SolidSamplesPresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleanerAddapproximately0.05gof***GraphitePowdertoa***GraphiteCrucible.Firmlyplacethecrucibleonthelowerelectrodetiporappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically**的動態(tài)流量補(bǔ)償(DFC)保證熱導(dǎo)池氣體流量、壓力恒定。山西專業(yè)分析儀廠家報(bào)價(jià)

Cornerstone氧氮?dú)浞治鲕浖瑫r(shí)支持***的數(shù)據(jù)文檔格式和可變的報(bào)告格式。專業(yè)元素分析儀

ONH836系列:氧氮?dú)浞治鰞x(熔融法)力可ONH836系列儀器采用惰性熔融法,提供各種無機(jī)材料、鋼鐵、有色金屬、硬質(zhì)合金、陶瓷材料中寬范圍的氧氮?dú)渫瑫r(shí)分析。ONH836系列儀器通過***采納客戶的反饋意見和創(chuàng)新設(shè)計(jì),力可***儀器采用觸摸屏技術(shù)和在線軟件平臺,增強(qiáng)了儀器的可操作性、降低了分析成本、節(jié)省實(shí)驗(yàn)室桌面空間。用戶友好界面的Cornerstone?軟件力可的Cornerstone氧氮氧分析軟件采用觸摸屏界面使用戶可完整的達(dá)到分析控制、方法設(shè)定、在線診斷、數(shù)據(jù)報(bào)告。Cornerstone氧氮氧分析軟件允許用戶在單一分析界面中完成日常的所有工作,快速而且簡單易用。力可創(chuàng)新的批次和重復(fù)樣品數(shù)據(jù)分組功能極大簡化了樣品結(jié)果輸出和結(jié)果標(biāo)準(zhǔn)偏差的自動計(jì)算,減少了繁瑣的額外數(shù)據(jù)處理。專業(yè)元素分析儀